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以下因為這次忘記拍照，先用一些示意圖，等之後修理其他支的機會，再來補照片
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The microtopography of HCNP is proven in Determine 2. The SEM and TEM effects clearly confirmed which the HCNP presents a spherical framework, and the diameter on the HCNP microsphere is about 2 um having a sleek surface.
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The microstructure review of your HCNP and char levels shaped in the combustion in the cone calorimetry examination was conducted utilizing the scanning electron microscope ZEISS Sigma HDTM. Illustrations or photos were being attained below vacuum at a voltage of five kV.
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Step 3, Specify Necessity Particulars: Enter the portion amount, maker and amount you call for from the provided fields. Deliver your standard tga66 Expense or goal price tag if relevant. Immediately after finishing all sections, post the shape by clicking the 'SUBMIT RFQ' button at the bottom appropriate.
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PA66 pellets and HCNP powder ended up dried for four h at a hundred °C before extrusion. The FR-PA66 was geared up by twin-screw extrusion response while in the array of 260–270 °C. The examination samples have been made using a TTI-95G injection molding equipment less than 265 °C by using a a hundred and eighty r/min rotation pace. Figure 6 reveals the microtopography of pure PA66, HCNP, and FR-PA66. It may be observed from Figure 6c that the HCNP microspheres had been dispersed additional uniformly devoid of noticeable period interfaces, as well as peeling phenomenon appeared about the surface area on the microspheres (Figure 6d), indicating which the terminal carboxyl groups of PA66 have been chemically bonded With all the amino teams about the floor of your microspheres through the extrusion reaction, which ruined the regularity in the area with the microspheres (Determine 6b, smooth surface and no peeling phenomenon) and led to your Main–shell separation of the microspheres (Determine 6d), confirming the event on the in situ loading reaction.